Nir spectroscopy ppt pdf

A free powerpoint ppt presentation displayed as a flash slide show on id. Ir spectroscopy or infrared spectroscopy is also called as vibrational spectroscopy. Pdf the continuous preference of the oral route for the delivery of the drugs has led. Spectroscopy is the study of the interaction of electromagnetic radiation with matter. Infrared spectroscopy ir theory and interpretation of ir spectra assigned readings introduction to technique 25 p. Nir spectroscopy is a desirable methodology due to its unique ability to measure a. The spectra observed in this region are primarily associated with the internal vibrational motion of molecules, but a few light molecules will have rotational transitions. Midir spectroscopy makes use of fundamental vibrations. Spectrophotometers were originally developed for the absorption measurement of liquid samples.

With emergence of nearinfrared spectroscopy nirs as a fast and nondestructive. Nir spectroscopy finds widespread use as an excellent. Ultravioletvisible spectroscopy uvvisnir optical design of 150 mm integrating sphere. Measurements in the ultravioletvisible region uvvis cover wavelengths from about 200 nm to 800 nm. Maywan hariono 2009 salycilic acid ethanol contoh spektrum allopurinol phenytoin references david g.

Nmr is a branch of spectroscopy and so it describes the nature of the energy levels of the material system and transitions induced between them through absorption or emission of electromagnetic radiation. In recent years, however, highprecision, highenergy spectrophotometers have hit the market due to the rapid increase in reflection and absorption measurements on solid samples, including semiconductors, films, glass, and. Spectroscopy is an instrumentally aided study of the interactions between matter sample being analyzed and energy any portion of the electromagnetic spectrum, ems introduction. This technique covers the region of the electromagnetic spectrum between the visible wavelength of 800 nanometres and the shortwavelength microwave 0. The nearinfrared portion of the electromagnetic spectrum is located between the visible and. Ultraviolet visible spectroscopy uvvisnir instrumentation. Near ir nuclear magnetic resonance nmr, raman, uvvisible uvvis. Davies norwich near infrared consultancy, 10 aspen way, cringleford, norwich nr4 6ua, uk. When you hold your hand out to a burning fire you feel the heat being emitted by the fire but what is happening. Microscope spectrophotometers or microspectrophotometersmsp are designed to measure uvvisnir spectra of microscopic samples or microscopic areas of larger objects.

The absorption of ultraviolet or visible radiation by a molecule leads to transitions among the electronic energy levels of. Huck this work shows that methods based on miniaturized near and midinfrared spectroscopy can be used. Raw materials identification testing by nir spectroscopy. Absorption spectroscopy techniques are covered in it and are used to recognize chemicals and study chemicals.

A guide to nearinfrared spectroscopic analysis of industrial manufacturing processes 5 1 preface nearinfrared spectroscopy nirs is a simple, quick 0 can absorbemit electromagnetic radiation. Em radiation in the ir and partially inmwrangedoesnotcarryenough energy to generate electronic excitation between two. This guideline outlines the requirements for applications in which nirs is used for qualitative and. Nearinfrared spectroscopy nir is a cost and timeeffective tool for evaluating the quality of feed. Excitation induces emission of light from the sample usually of different frequency. As nearinfrared nir spectroscopy and raman spectroscopy obtain spectra based on molecular vibrations, they both permit qualitative analysis. Near infra red spectroscopy an overview semantic scholar. Handbook of nearinfrared analysis, third edition uio. Infrared ir, atrir, mass spec ms, near infrared nir. An introduction to near infrared nir spectroscopy im. The collection of analytical techniques known as vibrational spectroscopy consists of three main tools, namely midinfrared or more commonly fourier transform infrared ftir. Market leading ccds, ingaas pdas, intensified ccds and electronmultiplying ccds for vuv to nir spectroscopy. Infrared ir spectroscopy is a powerful technique that allows to obtain information about the chemical structure of a variety of substances by utilizing infrared electromagnetic radiation.

The electromagnetic radiation may be anywhere from very high energy gamma rays to low. While a standard spectrophotometer is designed to measure samples on the order of 1 x 1 centimeters, the micro spectrophotometer is able to measure samples on the order of 1 x 1. Guideline on the use of near infrared spectroscopy nirs. Theory and utility of ftnir spectroscopy an introduction to nicolet. An introduction to optical spectroscopy by andrew hind. Near infrared spectroscopy nir is a type of vibrational.

Introduction to infrared ir spectroscopy basics and. Fluorescence emission from excited electronic singlet states phosphorescence emission from excited electronic triplet states raman scattering light scattering involving vibrational transition. The term near infrared indicates light with wavelengths between 800 nm and 2500 nm 12500 to 4000 cm 1 wavenumber. Spectroscopy spectroscopy is the study of the interaction between matter and radiated energy. Such transitions are forbidden by the selection rules of quantum mechanics. Nir spectroscopy a guide to nearinfrared spectroscopic. Ppt infrared spectroscopy powerpoint presentation free. Absorption appearing in the nearinfrared region involves overlaid harmonic and. It implicates an interaction of infrared radiation with matter. Nearinfrared spectroscopy is based on molecular overtone and combination vibrations. Ir absorption, raman, fluorescence and mass spectroscopy. Ir absorption, raman, fluorescence and mass spectroscopy g.